تفاعل #7642

ord-fea17c083a1e486d9dd4e00e7e5ed49c

معادلة التفاعل

CCC(N)c1nnc(-c2cccc([N+](=O)[O-])c2)[nH]c1=O
6-(1-aminopropyl)-3-(3-nitrophenyl)-1,2,4-triazin-5(4H)-one
O=C(Cl)C1CCCC1
cyclopentanecarbonyl chloride
CCC(NC(=O)C1CCCC1)c1nnc(-c2cccc([N+](=O)[O-])c2)[nH]c1=O
N-{1-[3-(3-Nitrophenyl)-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl]propyl}cyclopentanecarboxamide

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

In analogy to the procedure for Example 36A, 3.0 g (10.9 mmol) 6-(1-aminopropyl)-3-(3-nitrophenyl)-1,2,4-triazin-5(4H)-one, 2.2 g (16.3 mmol) cyclopentanecarbonyl chloride and proportionate amounts of the other reagents are used.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07087605B2uspto-grants-2006_08