تفاعل #75291
ord-3d92c6ce28bb4247ba978dfcc6f0040c
معادلة التفاعل
pyridine
phenacyl bromide
→
N-phenacylpyridinium bromide
المتفاعلات
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىThe slightly exothermic reaction
- 2أخرىwas accompanied by the precipitation of the solid N-phenacylpyridinium bromide
- 3ترشيحThe salt was then filtered
- 4غسيلwashed thoroughly with anhydrous ether
الإجراء التجريبي
N-phenacylpyridinium bromide was prepared by slowly adding phenacyl bromide to a stirred flask containing an equimolar quantity of pyridine. The slightly exothermic reaction was accompanied by the precipitation of the solid N-phenacylpyridinium bromide. The salt was then filtered and washed thoroughly with anhydrous ether.