تفاعل #75291

ord-3d92c6ce28bb4247ba978dfcc6f0040c

معادلة التفاعل

c1ccncc1
pyridine
O=C(CBr)c1ccccc1
phenacyl bromide
O=C(C[n+]1ccccc1)c1ccccc1.[Br-]
N-phenacylpyridinium bromide

المتفاعلات

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىThe slightly exothermic reaction
  2. 2
    أخرىwas accompanied by the precipitation of the solid N-phenacylpyridinium bromide
  3. 3
    ترشيحThe salt was then filtered
  4. 4
    غسيلwashed thoroughly with anhydrous ether

الإجراء التجريبي

N-phenacylpyridinium bromide was prepared by slowly adding phenacyl bromide to a stirred flask containing an equimolar quantity of pyridine. The slightly exothermic reaction was accompanied by the precipitation of the solid N-phenacylpyridinium bromide. The salt was then filtered and washed thoroughly with anhydrous ether.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US04175973uspto-grants-1979_11