تفاعل #75255

معادلة التفاعل

product

Ethyl 4-(4-Acetyl-8-acetoxy-9-propoxynonyl)benzoate

ethyl 4-(4-acetyl-8-acetoxytridecyl)benzoate

→

4-(4-Acetyl-8-hydroxy-9-propoxynonyl)benzoic Acid

ظروف التفاعل

المعالجة

1. 1
   أخرىThis compound is prepared by the method
2. 2
   أخرىThe title compound is purified by column chromatography on silica gel with 4% methanol in chloroform as the eluant

الإجراء التجريبي

This compound is prepared by the method described in Example 1, Step F, except that the product of Step C of the present example replaces ethyl 4-(4-acetyl-8-acetoxytridecyl)benzoate. The title compound is purified by column chromatography on silica gel with 4% methanol in chloroform as the eluant. The title compound is a light yellow, viscous oil.

المصدر