تفاعل #75020
ord-3382055977444d27a94c974baede3424
معادلة التفاعل
Styrene
acetic acid
→
gamma-phenyl butyrolactone
المردود 70.0%
المتفاعلات
الكواشف
لا شيء
ظروف التفاعل
درجة الحرارة
110°CELSIUS
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
Styrene in the amount of 20 grams was dissolved in 100 milliliters of acetic acid containing 10% potassium acetate. Ceric acetate in the amount of 0.005 mole was added and the reaction mixture was heated in a sealed tube at 110° C. overnight. The lactone, gamma-phenyl butyrolactone, was obtained in 70% yield.