تفاعل #74698
ord-222aa578598c45ddb5e533f9892fe67c
معادلة التفاعل
5-(4-Methoxyphenylazo)salicoyl chloride
6-aminobenzimidazole
→
N-(benzimidazol-6-yl)-2-hydroxy-5-(4-methoxyphenylazo)benzamide
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىas described for Preparation 7
- 2أخرىThe product was crystallized in aqueous pyridine
الإجراء التجريبي
5-(4-Methoxyphenylazo)salicoyl chloride and 6-aminobenzimidazole were reacted together as described for Preparation 7. The product was crystallized in aqueous pyridine, m.p. 274°, λmax (methanol)=350 nm.