تفاعل #742273

ord-b1dbd61695ec42a4809475f3bb8c1881

معادلة التفاعل

O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
CCN(CC)CC
triethylamine
O=S(=O)(O)C(F)(F)F
trifluoromethanesulfonic acid
CCN(CC)CC
triethylamine
CC[NH+](CC)CC.O=S(=O)([O-])C(F)(F)F
triethylammonium trifluoromethanesulfonate

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    درجة الحرارةwhile being cooled by liquid nitrogen
  2. 2
    أخرىthus obtaining a target ionic conductor

الإجراء التجريبي

Equimolar amounts of triethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed triethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US08071253B2uspto-grants-2011_12