تفاعل #742254

ord-581177628e1f4b01b4e20ea1b76dd49d

معادلة التفاعل

CCC(=CCC1CC=C(C)C1(C)C)COC(=O)C=Cc1cc(C)ccc1O
3-(2-hydroxy-5-methyl-phenyl)-acrylic acid 2-ethyl-4-(2,2,3-trimethyl-cyclopent-3-enyl)-but-2-enyl ester
CCOC(=O)C=Cc1cc(C)ccc1O
3-(2-hydroxy-5-methyl-phenyl)-acrylic acid ethyl ester
CCC(=CCC1CC=C(C)C1(C)C)COC(=O)/C=C/c1cc(C)ccc1O
(E)-3-(2-Hydroxy-5-methyl-phenyl)-acrylic acid 2-ethyl-4-(2,2,3-trimethyl-cyclopent-3-enyl)-but-2-enyl ester

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

According to the same procedure, 3-(2-hydroxy-5-methyl-phenyl)-acrylic acid 2-ethyl-4-(2,2,3-trimethyl-cyclopent-3-enyl)-but-2-enyl ester was prepared from 3-(2-hydroxy-5-methyl-phenyl)-acrylic acid ethyl ester, 2-ethyl-4(2,2,3-trimethyl cyclopentyl-3-en-1-yl)-but-2-en-1-ol and tetraisopropyl-o-titanate.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: USRE043006E1uspto-grants-2011_12