تفاعل #734413

معادلة التفاعل

1-(2,5-dichlorophenylazo)-5-(m-dioctadecylcarbamoylbenzenesulfonamido)-2-naphthol

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1-Amino-5-(m-dioctadecylcarbamoylbenzenesulfonamido)-2-naphthol

ظروف التفاعل

المعالجة

1. 1
   ترشيحThe catalyst was filtered
2. 2
   أخرىthe solution kept under nitrogen during its immediate use in the above reaction

الإجراء التجريبي

A mixture of the azo dye, 1-(2,5-dichlorophenylazo)-5-(m-dioctadecylcarbamoylbenzenesulfonamido)-2-naphthol (10.2 g, 0.01 mol) and 10 percent palladium on carbon (1.5 g) was hydrogenated at 40 psi and room temperature for 2 hours. The catalyst was filtered and the solution kept under nitrogen during its immediate use in the above reaction.

المصدر