تفاعل #720258

معادلة التفاعل

3-chloro-4-(4-chloro-3-(pyridin-2-yl)phenylcarbamoyl)benzoic acid

diethylamine hydrochloride

→

2-chloro-N1-(4-chloro-3-(pyridin-2-yl)phenyl)-N4,N4-diethylterephthalamide

ظروف التفاعل

المعالجة

1. 1
   أخرىThe product was purified on reverse phase HPLC

الإجراء التجريبي

75 mg of 3-chloro-4-(4-chloro-3-(pyridin-2-yl)phenylcarbamoyl)benzoic acid was coupled to diethylamine hydrochloride via Procedure G. The product was purified on reverse phase HPLC to yield 2-chloro-N1-(4-chloro-3-(pyridin-2-yl)phenyl)-N4,N4-diethylterephthalamide. MS (Q1) 443 (M)+.

المصدر