تفاعل #71585
ord-9a99f6c83ecb45f2a14080de6416e4b9
معادلة التفاعل
ethyl tiglate
thioacetic acid
ethyl tiglate
→
ethyl 3-acetylthio-2-methylbutyrate
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىwas prepared
- 2أخرىto react under nitrogen atmosphere at 85° C. for 24 hours
الإجراء التجريبي
A mixture of 3.20 g (0.025 mol) of ethyl tiglate and 4.76 g (0.0625 mol) of thioacetic acid was prepared and allowed to react under nitrogen atmosphere at 85° C. for 24 hours. The results showed that the conversion rate of ethyl tiglate was 35.3%, and that the selectivity for the objective compound was 91.6%.