تفاعل #709801
ord-dc46182844334b19941924c42a7251fd
المتفاعلات
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1workup.ADDITIONwas dropwise added
- 2ترشيحthe reaction mixture was filtered
الإجراء التجريبي
4-Cyanostilbene (41 g) prepared by a known method was agitated in 300 ml of ether at room temperature, to which 33.5 g of bromine was dropwise added. After stirred for additional one hour, the reaction mixture was filtered to obtain 55.5 g of 4-cyanostilbene dibromide.