تفاعل #709801

ord-dc46182844334b19941924c42a7251fd

المتفاعلات

الكواشف

لا شيء

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    workup.ADDITIONwas dropwise added
  2. 2
    ترشيحthe reaction mixture was filtered

الإجراء التجريبي

4-Cyanostilbene (41 g) prepared by a known method was agitated in 300 ml of ether at room temperature, to which 33.5 g of bromine was dropwise added. After stirred for additional one hour, the reaction mixture was filtered to obtain 55.5 g of 4-cyanostilbene dibromide.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US04772534uspto-grants-1988_09