تفاعل #70978

ord-e53f4ee389a449ed958feb11973d33af

معادلة التفاعل

CCSc1c(C=O)c(=O)n(C)c(=O)n1C
6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde
Cl.NOCc1ccccc1
O-benzyl-hydroxylamine hydrochloride
CCSc1c(C=NOCc2ccccc2)c(=O)n(C)c(=O)n1C
title compound
CCSc1c(C=NOCc2ccccc2)c(=O)n(C)c(=O)n1C
6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde O-benzyloxime

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

The process described in Method A was followed. 6-(Ethylthio)-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (Example 23, Step 1) (0.070 mg, 0.30 mmol) and O-benzyl-hydroxylamine hydrochloride (0.063 mg, 0.40 mmol) were used to obtain the title compound.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US08536210B2uspto-grants-2013_09