تفاعل #70972

ord-5421e4db7618452e8854aebe29cfa64a

معادلة التفاعل

CCOc1c(C=O)c(=O)n(C)c(=O)n1C
6-Ethoxy-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde
Cl.NOCc1ccccc1
O-benzyl-hydroxyl-amine hydrochloride
CCOc1c(C=NOCc2ccccc2)c(=O)n(C)c(=O)n1C
title compound
CCOc1c(C=NOCc2ccccc2)c(=O)n(C)c(=O)n1C
6-Ethoxy-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde O-benzyloxime

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

The process described in Method A was followed. 6-Ethoxy-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.074 mg, 0.35 mmol) (Example 16, Step 1) and O-benzyl-hydroxyl-amine hydrochloride (0.073 mg, 0.46 mmol) were used to obtain the title compound.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US08536210B2uspto-grants-2013_09