تفاعل #70344
ord-173a0ffe83b349cd963070606fb7fc29
معادلة التفاعل
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىThe solvent was evaporated
- 2أخرىthe residue was triturated in diethyl ether
- 3أخرىThe solid formed
- 4ترشيحwas filtered off
- 5أخرىto afford
الإجراء التجريبي
A solution of 5-methyl-2-(6-morpholinopyridin-3-ylamino)benzoate tert-butyl ester in TFA (0.6 ml, 7.58 mmol) was stirred at room temperature for 1 hour. The solvent was evaporated and the residue was triturated in diethyl ether. The solid formed was filtered off to afford 0.047 g (73% of yield) of the expected product.