تفاعل #70034
ord-225648086b724bd2b3dbff6a448ccb30
معادلة التفاعل
1-isocyano-2-methylpropan-2-yl methyl carbonate
1H-benzo[d]imidazol-5-amine
4-thiomorpholinobenzaldehyde
sodium tert.-butoxide
2-(ethoxycarbonyl)acetic acid
→
1-(1H-Benzo[d]imidazol-5-yl)-5-(4-thiomorpholinophenyl)-pyrrolidine-2,4-dione
المتفاعلات
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىThe compound was synthesized
الإجراء التجريبي
The compound was synthesized starting from 1H-benzo[d]imidazol-5-amine (0.963 g, 7.24 mmol), 4-thiomorpholinobenzaldehyde (1.5 g, 7.24 mmol), 2-(ethoxycarbonyl)acetic acid (0.957 g, 7.24 mmol), 1-isocyano-2-methylpropan-2-yl methyl carbonate (1.13 g, 7.24 mmol) and sodium tert.-butoxide (0.77 g, 6.87 mmol) according to method 3.