تفاعل #68859

معادلة التفاعل

6-chloro-2-methyl-quinoline

1,4-dioxane

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title compound

6-Chloro-quinoline-2-carbaldehyde

ظروف التفاعل

المعالجة

1. 1
   ترشيحThe resulting black mixture was filtered through diatomaceous earth

الإجراء التجريبي

A suspension of 6-chloro-2-methyl-quinoline (355 mg) and SeO2 (233 mg) in 1,4-dioxane (3 mL) was heated at 80° C. for 16 h. The resulting black mixture was filtered through diatomaceous earth. Concentration of the filtrate gave the title compound as a yellow powder (324 mg).

المصدر