تفاعل #67825

ord-9a704c2cf2a74393a9bd3da4929cb2e2

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىLC/MS [8.99 min; 455 (M+1)]

الإجراء التجريبي

N-azepan-1-yl-3-[(2-fluoro-4-iodophenyl)amino]isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.45 mmol of 3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid (intermediate 1) and 6.2 mmol of azepan-1-ylamine. LC/MS [8.99 min; 455 (M+1)]

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US08524911B2uspto-grants-2013_09