تفاعل #66961

معادلة التفاعل

3-Bromo-4-methoxyphenylacetic acid

EtOH

→

title compound

(3-Bromo-4-methoxy-phenyl)-acetic acid ethyl ester

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةAfter cooling to room temperature
2. 2
   تركيزthe mixture was concentrated

الإجراء التجريبي

3-Bromo-4-methoxyphenylacetic acid (4.1 g, 16.7 mmol) in EtOH (100 mL) was treated with concentrated HCl (2 drops) and heated to 80° C. for 3 days. After cooling to room temperature, the mixture was concentrated to give the title compound.

المصدر