تفاعل #66939

معادلة التفاعل

167

Dibenzyl 2-(3-([bis-[(benzyl)oxy]]phosphoryl)oxy-5-methoxyphenyl) -6,7-methylenedioxyquinolin-4-yl phosphate

→

168

المردود 45.0%

2-(3-([bis-[(benzyl)oxy]]phosphoryl)oxy-5-methoxyphenyl)-6,7-methylenedioxyquinolin-4-one

المردود 45.0%

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   أخرىThe precipitates were collected
2. 2
   أخرىpurified by column chromatography (SiO2, EtOAc)

الإجراء التجريبي

A suspension of 0.92 g (1.11 mmol) of 167 in 100 mL of methanol was stirred at 25° C. for 48 h. The precipitates were collected and purified by column chromatography (SiO2, EtOAc) to give 168.

المصدر