تفاعل #6683

معادلة التفاعل

[R]-1-trifluoromethylheptyl 4-benzyloxybenzoate

→

[R]-1-Trifluoromethylheptyl 4-hydroxybenzoate

المردود 99.0%

المذيبات

ethyl acetate

ظروف التفاعل

المعالجة

1. 1
   ترشيحThen the catalyst was filtered out
2. 2
   أخرىfiltrate was evaporated to dryness
3. 3
   أخرىto give the pure compound in yield of 99%

الإجراء التجريبي

2.2 g of [R]-1-trifluoromethylheptyl 4-benzyloxybenzoate, (13) 100 mg of PdOH/C in 50 ml of ethyl acetate was stirred at RT over night under H2 atmosphere. Then the catalyst was filtered out and filtrate was evaporated to dryness to give the pure compound in yield of 99%.

المصدر