تفاعل #66590

معادلة التفاعل

Iodomethane

3-((dimethylamino)methyl)-5-methylhexan-2-one

→

title product

المردود 68.4%

(2-Acetyl-4-methyl-pentyl)-trimethyl-ammonium iodide

المردود 68.4%

المذيبات

ethyl acetate

ظروف التفاعل

المعالجة

1. 1
   ترشيح, and the resulting preciptant was collected by filtration

الإجراء التجريبي

Iodomethane (20 g, 140.94 mmol, 2.00 equiv) was added dropwise to a solution of 3-((dimethylamino)methyl)-5-methylhexan-2-one (12 g, 70.05 mmol, 1.00 equiv) and ethyl acetate (50 mL). The solution was stirred at ambient temperature for about 16 hours., and the resulting preciptant was collected by filtration to afford the title product (15 g, yield=68%).

المصدر