تفاعل #66010

معادلة التفاعل

allyl bromide

diethylene glycol

→

Diethylene glycol monoallyl ether

المردود 82.0%

المذيبات

THF NaH

ظروف التفاعل

المعالجة

1. 1
   أخرىThe product was obtained in 82% yield
2. 2
   workup.DISTILLATIONafter distillation

الإجراء التجريبي

Diethylene glycol monoallyl ether was prepared by reacting allyl bromide with excess diethylene glycol in THF-NaH (tetrahydrofuran-sodium hydride). The product was obtained in 82% yield after distillation. b.p.=96-99° C./7 mmHg.

المصدر