تفاعل #65300
ord-d714a4907e85428cb8eae91d6d2f93c7
معادلة التفاعل
chlorotrimethylsilane
Chlorotrifluoroethylene
n-butyl lithium
→
1,1,2-trifluoro-2-trimethylsilylethylene
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
Chlorotrifluoroethylene of the formula (10) is treated with n-butyl lithium and then reacted with chlorotrimethylsilane of the formula (11) to obtain 1,1,2-trifluoro-2-trimethylsilylethylene of the formula (12). Then, without isolation, this compound (12) is reacted further with a lithium compound of the formula (13) to obtain a difluoroethylene compound of the formula (14).