تفاعل #64954

معادلة التفاعل

6-benzyl-1-methyl-octahydropyrrolo[3,4-b]pyridine

dihydrochloride

→

1-Methyl-octahydropyrrolo[3,4-b]pyridine

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   workup.DISTILLATIONWorking up by distillation
2. 2
   أخرىgives 2.6 g (34% of theory) of a colorless oil of boiling point 83°-85°/12 mbar)

الإجراء التجريبي

11.7 g (54 retool) of 6-benzyl-1-methyl-octahydropyrrolo[3,4-b]pyridine as the dihydrochloride are hydrogenated in 100 ml of methanol over palladium-on-active charcoal in accordance with the working instructions of Example Id. Working up by distillation gives 2.6 g (34% of theory) of a colorless oil of boiling point 83°-85°/12 mbar).

المصدر