تفاعل #64287

معادلة التفاعل

ethanol

5'-methylspiro[1-azabicyclo[2,2,2]-octane-3,2'-thiolan]-4'-one

hydrochloride

hydrogen chloride

→

5'-Methyl-4'-methylenespiro[1-azabicyclo[2,2,2]-octane-3,2'-thiolane]

ظروف التفاعل

الإجراء التجريبي

5'-Methyl-4'-methylenespiro[1-azabicyclo[2,2,2]-octane-3,2'-thiolane] was prepared in much the same manner as in Example 5 by using 5'-methylspiro[1-azabicyclo[2,2,2]-octane-3,2'-thiolan]-4'-one. It was dissolved in ethanol, and then convereted to hydrochloride by addition of ethanolic hydrogen chloride.

المصدر