تفاعل #64238

ord-65c05d3a7c4048fa95c6e4a60246683b

معادلة التفاعل

O=C(O)c1ccc(C(=O)OCc2ccccc2)cc1
4-benzyloxycarbonylbenzoic acid
CCN(CC)CCN
N,N-diethylethylene diamine
CCN(CC)CCNC(=O)c1ccc(C(=O)O)cc1
4-([2-(N,N-diethylamino)ethyl]aminocarbonyl)benzoic acid

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

4-([2-(N,N-diethylamino)ethyl]aminocarbonyl)benzoic acid was prepared from 4-benzyloxycarbonylbenzoic acid by reaction with N,N-diethylethylene diamine to yield the mono amide derivative which was hydrogenolysed to give the acid (CI-MS: m/z 265 [M+b]+).

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US05411984uspto-grants-1995_05