تفاعل #640569

معادلة التفاعل

diethyl ether

thioanisole

dimethyl sulfate

→

dimethylphenylsulfonium sulfate

المذيبات

water

water

ظروف التفاعل

الإجراء التجريبي

At room temperature, 6.2 g (0.05 mole) of thioanisole and 6.9 g (0.055 mole) of dimethyl sulfate were stirred for 12 hours. To the reaction solution were added 100 g of water and 50 ml of diethyl ether. The water layer was taken out, obtaining an aqueous solution of the desired dimethylphenylsulfonium sulfate.

المصدر