تفاعل #640563
ord-c83f9a78c34a455c8b29550583c48eaa
معادلة التفاعل
2-aminophenylboronic acid
acryloyl chloride
→
2-Acrylamido-phenylboronic acid
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1استخلاصThe product was extracted in acetone
- 2أخرىdried
- 3أخرىa rotary evaporator
الإجراء التجريبي
2-Acrylamido-phenylboronic acid (“2-APB”) was synthesized by reacting 2-aminophenylboronic acid with an excess of acryloyl chloride in an aqueous alkaline solution. The product was extracted in acetone and dried using a rotary evaporator. The structure of 2-APB was confirmed using NMR. The purity was shown to be greater than 90%.