تفاعل #63288
ord-5116b757d2fc4b29bf10d174261fb24e
معادلة التفاعل
N-[1-(4-methoxyphenyl)-3-piperidinopropyl]quinaldinamide
oxalic acid dihydrate
→
subject compound
المردود 70.0%
N-[1-(4-methoxyphenyl)-3-piperidinopropyl]quinaldinamide oxalate
المردود 70.0%
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
The procedure of Example 7 was repeated using 1.03 g (2.56 mmol.) of N-[1-(4-methoxyphenyl)-3-piperidinopropyl]quinaldinamide and 323 mg (2.56 mmol.) of oxalic acid dihydrate, to obtain 884 mg (yield: 70%) of the subject compound as a white powdery product upon recrystallization from 8 ml of ethanol.