تفاعل #63223

معادلة التفاعل

5-bromo-2-furancarboxylic acid

thionyl chloride

→

5-bromo-2-furancarboxylic acid chloride

المذيبات

toluene

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةto reflux for 2 hours
2. 2
   تركيزThe reaction solution was thereafter concentrated

الإجراء التجريبي

21.0 g of 5-bromo-2-furancarboxylic acid were suspended in 650 ml of toluene and 40 ml of thionyl chloride and the suspension was heated to reflux for 2 hours. The reaction solution was thereafter concentrated, whereby 5-bromo-2-furancarboxylic acid chloride was obtained as the residue.

المصدر