تفاعل #631975
ord-55cefff41d0346b1bd2437b3200c3d54
معادلة التفاعل
6-hydroxy-2-naphthyl benzoate
nitric acid
water
→
6-hydroxy-5-nitro-2-naphthyl benzoate
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىat 15° C.
- 2أخرىThe thus obtained deposit was recrystallized from ethanol/acetic acid
الإجراء التجريبي
The thus obtained 6-hydroxy-2-naphthyl benzoate was dispersed in acetic acid, nitric acid was added dropwise to the dispersion while keeping it at 15° C., and water was further added thereto, followed by stirring. The thus obtained deposit was recrystallized from ethanol/acetic acid to obtain 6-hydroxy-5-nitro-2-naphthyl benzoate.