تفاعل #62787

معادلة التفاعل

Dichloromaleic anhydride

Bis-(3-chloroallyl)amine

→

above-named product

المردود 99.1%

N,N-bis-(3-chloroallyl) dichloromaleic monoamide

المردود 99.1%

المذيبات

methylene chloride

ظروف التفاعل

المعالجة

1. 1
   أخرىThe exothermic reaction
2. 2
   أخرىyielded a clear solution

الإجراء التجريبي

Dichloromaleic anhydride (1.7 g, 0.01 mol) and 30 ml methylene chloride were stirred under a mild reflux. Bis-(3-chloroallyl)amine (1.7 g, 0.01 mol) was then added. The exothermic reaction yielded a clear solution. The solution was stirred at room temperature for 3 hours. The mixture was stripped, resulting in 3.3 g of the above-named product.

المصدر