تفاعل #62536

ord-5046a917121f46f6b069f9070b68db87

الكواشف

لا شيء

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىwas kept at 40° C.
  2. 2
    أخرىremoved from the resulting emulsion by pH-adjustment

الإجراء التجريبي

In 3,000 ml of water were dissolved 28 g of gelatin and 13.2 g of benzotriazole, and the solution was kept at 40° C. while stirring. To the solution was added 100 ml of an aqueous solution of 17 g of silver nitrate over 2 minutes. Excessive salts were sedimented and removed from the resulting emulsion by pH-adjustment. Thereafter, the emulsion was adjusted to pH 6.30 to obtain a silver benzotriazole emulsion. The yield of the emulsion was 400 g.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US04761360uspto-grants-1988_08