تفاعل #61363

ord-58af42bff0d2471f923fbfc26427f07e

معادلة التفاعل

Cl.Cl.Nc1c(F)c(N)c(F)c(F)c1F
dihydrochloride
O=[N+]([O-])c1ccc(NCCc2cccs2)cc1
N-(4-nitrophenyl)-N-(2-thien-2-ylethyl)amine
Cl.Cl.Nc1ccc(NCCc2cccs2)cc1
amine
Cl.Cl.Nc1ccc(NCCc2cccs2)cc1
N-(2-thiophen-2-ylethyl)benzene-1,4-diamine dihydrochloride

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

The N-(4-nitrophenyl)-N-(2-thien-2-ylethyl)amine (1) obtained above was reduced with a boiling zinc/ammonium chloride/water/ethanol mixture. The corresponding amine was isolated in dihydrochloride form.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07429278B2uspto-grants-2008_09