تفاعل #61206

ord-b5540e30025645ddba03804710f0b6db

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىThis compound-was prepared

الإجراء التجريبي

This compound-was prepared using the general Sonagashira conditions as described in general Example C, starting from N-(2-iodo-4-nitro-5-trifluoromethyl-phenyl)-methanesulfonamide (9.0 g, 21.9 mmol) and 2-methyl-1-buten-3-yne (6.25 mL, 65.7 mmol) to yield the title compound as a reddish-brown solid.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07427682B2uspto-grants-2008_09