تفاعل #6109
ord-be2199f40d44415e9d6c4b76de61d7c9
معادلة التفاعل
dimethylthiocarbamoyl chloride
2-tri-fluoromethylphenol
potassium hydroxide
→
yellow oil
المردود 89.0%
O-2-trifluoromethylphenyl dimethylthiocarbamate
المردود 89.0%
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
If the procedure described in Preparation XI is followed starting from 3.95 g (24.3.10-3 mol) of 2-tri-fluoromethylphenol, 1.43 g (25.6.10-3 mol) of potassium hydroxide and 3.46 g (28.10-3 mol) of dimethylthiocarbamoyl chloride, 5.37 g (yield: 89%) of a yellow oil are obtained.