تفاعل #6100
ord-0e3bf4991a3f466d9c41ae0105fc4554
معادلة التفاعل
potassium hydroxide
2-hydroxybenzonitrile
dimethylthiocarbamoyl chloride
→
expected product
المردود 94.0%
O-2-cyanophenyl dimethylthiocarbamate
المردود 94.0%
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
If the procedure described in Preparation XVI is followed starting from 15 g (126.10-3 mol) of 2-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (126.10-3 mol) of potassium hydroxide, 24.1 g (yield: 94%) of the expected product are obtained.