تفاعل #60556

معادلة التفاعل

1-nitro-2-(3,3,5,5-tetramethylcyclohex-1-enyl)benzene

hydrogen

→

2-(3,3,5,5-Tetramethylcyclohexyl)phenylamine

المذيبات

ethyl alcohol

ظروف التفاعل

المعالجة

1. 1
   أخرىwas placed in a flask
2. 2
   أخرىReaction
3. 3
   أخرىunder the same reaction conditions
4. 4
   أخرىThe three reaction mixtures

الإجراء التجريبي

A mixture of 1-nitro-2-(3,3,5,5-tetramethylcyclohex-1-enyl)benzene (130.0 g, 501.3 mmol), 10% palladium on carbon (13.0 g, wet) and ethyl alcohol (1820 mL) was placed in a flask, then the inside of the flask was replaced with hydrogen, and the mixture was stirred for 78 hours at room temperature under a hydrogen atmosphere at atmospheric pressure. Reaction was repeated two more times on the same scale as above, by the same procedure under the same reaction conditions. The three reaction mixtures were combined and subjected to the following treatment.

المصدر