تفاعل #595369

معادلة التفاعل

methyl 4-(benzyloxy)-2-(prop-1-en-2-yl)benzoate

→

title compound

methyl 4-hydroxy-2-isopropylbenzoate

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   ترشيحThen the mixture was filtered
2. 2
   تركيزthe filtrate was concentrated

الإجراء التجريبي

To a solution of methyl 4-(benzyloxy)-2-(prop-1-en-2-yl)benzoate (i-1d) (4.6 g, 16.3 mmol) in methanol (100 ml) was added Pd/C (0.46 g). The mixture was stirred at rt under H2 atmosphere for 24 h. Then the mixture was filtered, and the filtrate was concentrated to afford the title compound. LCMS (ESI) calc'd for C11H14O3 [M+H]+: 195.1. found: 195.1.

المصدر