تفاعل #58756

معادلة التفاعل

6-bromo-pyridine-2-carbaldehyde

2-methoxy-ethylamine

→

title compound

المردود 94.0%

(6-Bromo-pyridin-2-ylmethyl)-(2-methoxy-ethyl)-amine

المردود 94.0%

ظروف التفاعل

المعالجة

1. 1
   أخرىThe title compound was prepared in a manner similar to
2. 2
   أخرىThe crude product was purified (SiO2: 0-5% MeOH/DCM)

الإجراء التجريبي

The title compound was prepared in a manner similar to that described in Example 18, Step C, using 6-bromo-pyridine-2-carbaldehyde (0.275 g, 1.48 mmol) and 2-methoxy-ethylamine (0.111 g, 1.48 mmol). The crude product was purified (SiO2: 0-5% MeOH/DCM) to yield the title compound (0.34 g, 94%).

المصدر