تفاعل #5843

ord-1bf8d60c367e45b9942d7471cdaae72c

معادلة التفاعل

[I-]
iodide
N[C@@H](Cc1ccc(O)c(I)c1)C(=O)O
3-iodo-L-tyrosine
[I-]
iodide
N[C@@H](Cc1ccc(O)cc1)C(=O)O
Tyrosine

المتفاعلات

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

Electrolysis was carried out using the same cell, anode, membrane and procedure as in Example 15, except that the pH of the anolyte and catholyte was 7.0. At 85% iodide conversion, the yield of 3-iodo-L-tyrosine was 58% based on initial iodide.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US05246561uspto-grants-1993_09