تفاعل #583967

معادلة التفاعل

g-butyrolactone

n-butylamine

→

N-butyl-4-hydroxybutyramide

ظروف التفاعل

المعالجة

1. 1
   أخرىthe excess n-butylamine was removed in vacuo
2. 2
   أخرىThe product crystallized
3. 3
   أخرىto give about 62 g of a colorless,

الإجراء التجريبي

To 30 mL (390 mmol) of g-butyrolactone was added 45 ml (455 mmol) of n-butylamine. The solution was heated at 85° C. for 1.5 hr, then the excess n-butylamine was removed in vacuo. The product crystallized on standing to give about 62 g of a colorless, low melting solid.

المصدر