تفاعل #58261

ord-67d0165016824c9f88d8389d83c0600b

معادلة التفاعل

COc1ccc(C(=O)c2ccc3c(c2)OCO3)c(C(=O)O)c1
2-(1,3-benzodioxol-5-yl)carbonyl-5-methoxybenzoic acid
NN.O
hydrazine hydrate
→
COc1ccc2c(-c3ccc4c(c3)OCO4)n[nH]c(=O)c2c1
4-(1,3-Benzodioxol-5-yl)-7-methoxy-2H-phthalazin-1-one

المتفاعلات

COc1ccc(C(=O)c2ccc3c(c2)OCO3)c(C(=O)O)c1
2-(1,3-benzodioxol-5-yl)carbonyl-5-methoxybenzoic acid
NN.O
hydrazine hydrate

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىThis compound is obtained

الإجراء التجريبي

This compound is obtained according to the procedure described in 1.2. by reacting 2-(1,3-benzodioxol-5-yl)carbonyl-5-methoxybenzoic acid unpurified with hydrazine hydrate.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07423030B2uspto-grants-2008_09