تفاعل #579448

معادلة التفاعل

tetrahydrothiophene

1-bromo-3,3-dimethyl-2-butanone

→

1-(3,3-dimethyl-2-oxobutyl)tetrahydrothiophenium bromide

المذيبات

acetone

ظروف التفاعل

المعالجة

1. 1
   workup.ADDITIONwas added dropwise
2. 2
   أخرىwhite solid obtained
3. 3
   ترشيحwas filtered
4. 4
   غسيلwashed with acetone
5. 5
   أخرىdried

الإجراء التجريبي

70.2 Parts of tetrahydrothiophene was dissolved in 750 parts of acetone, and 150 parts of 1-bromo-3,3-dimethyl-2-butanone was added dropwise thereto. After the mixture was stirred at room temperature for 24 hours, white solid obtained was filtered, washed with acetone and dried to obtain 161.3 parts of 1-(3,3-dimethyl-2-oxobutyl)tetrahydrothiophenium bromide in the form of white crystals.

المصدر