تفاعل #564248

ord-7cf1c8d830fe483db8fd085ee7f9672d

معادلة التفاعل

C[O-].[Na+]
sodium methoxide
O=C(OCC(O)CO)c1ccccc1O
glycerol salicylate
CC(CO)(CO)CO
trimethylolethane
COC(=O)c1ccccc1O
methyl salicylate
COC(=O)c1ccccc1O
methyl salicylate
CC(CO)(CO)CO.O=C(O)c1ccccc1O
Trimethylolethane salicylate

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

Trimethylolethane salicylate was prepared by the method described in Example 1 for the preparation of glycerol salicylate except that the reactants were trimethylolethane (60.1 g; 0.5 moles), methyl salicylate (119.7 g; 0.788 moles), sodium methoxide (0.82 g; 0.015 moles). The final methyl salicylate level was 10.0%.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US04886843uspto-grants-1989_12