تفاعل #55656

معادلة التفاعل

3-nitro-4-chloro-benzophenone

N-ethyl-N-cyclohexylamine

→

3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone

ظروف التفاعل

المعالجة

1. 1
   أخرىThe crude product is recrystallized from n-hexane

الإجراء التجريبي

13 g. of 3-nitro-4-chloro-benzophenone are reacted with 15 ml. of N-ethyl-N-cyclohexylamine as described in Example 2. The crude product is recrystallized from n-hexane to yield 15.3 g of pure, crystalline 3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone; m.p. 91.5°-92° C.

المصدر