تفاعل #55597

معادلة التفاعل

5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid

sodium hydroxide

→

product

المردود 105.4%

Sodium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate

المردود 105.4%

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   أخرىThe solvent is then removed in vacuo

الإجراء التجريبي

5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (1.7 g, 0.0047 mole) is dissolved in methanol (25 ml) and sodium hydroxide (4.7 ml of 1 N NaOH in methanol, 0.0047 mole) is added rapidly. The solvent is then removed in vacuo to give 1.9 g of product that decomposes at 217° C.

المصدر