تفاعل #554581
ord-956fe17f6170423684ccc3549d6672c7
معادلة التفاعل
5-(4-Isopropylphenyl)-2-methyl-1-pentanol
hydrogen
→
5-(4-isopropylcyclohexyl)-2-methyl-1-pentanol
المردود 99.7%
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىThe catalyst was removed
- 2workup.DISTILLATIONthe product distilled
الإجراء التجريبي
100 g of 5-(4-Isopropylphenyl)-2-methyl-1-pentanol (obtained as described in EP 0 908 439) combined with 1.5 g Ru on aluminium oxide (Ru content 5 wt. %) were hydrogenated at a hydrogen pressure of 25 bar and at a temperature of 110° C. After 15 hours the reaction was finished. The catalyst was removed and the product distilled. 100 g (content 99.7%) of 5-(4-isopropylcyclohexyl)-2-methyl-1-pentanol were obtained.