تفاعل #554124

معادلة التفاعل

1-(2-methoxymethoxyphenyl)-1-(4-methyl-2-methoxyphenyl)ethene

phenylthiomethyl lithium

→

title compound

المردود 44.0%

1-(2-Methoxymethoxyphenyl)-1-(4-methyl-2-methoxyphenyl)cyclopropane

المردود 44.0%

ظروف التفاعل

الإجراء التجريبي

The general procedure of Example 34 was followed using 1-(2-methoxymethoxyphenyl)-1-(4-methyl-2-methoxyphenyl)ethene and, initially, 3.3 moles of phenylthiomethyl lithium reagent per mole of olefin. The title compound was obtained as a clear oil in 44 percent yield and its structure was verified by proton NMR spectroscopy.

المصدر