تفاعل #54888

ord-78a9f11cb0714561a8b1dcedd5745f70

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىThis compound is prepared by the method
  2. 2
    أخرىThe title compound is purified by column chromatography on silica gel with 4% methanol in chloroform as the eluant

الإجراء التجريبي

This compound is prepared by the method described in Example 1, Step F, except that the product of Step C of the present example replaces ethyl 4-(4-acetyl-8-acetoxytridecyl)benzoate. The title compound is purified by column chromatography on silica gel with 4% methanol in chloroform as the eluant. The title compound is a light yellow, viscous oil.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US04150235uspto-grants-1979_04